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Beilstein J. Org. Chem. 2017, 13, 644–647, doi:10.3762/bjoc.13.63
Graphical Abstract
Scheme 1: Top: The natural product deoxynojirimycin and two analogues and marketed drugs Glyset and Zavesca. ...
Scheme 2: Synthesis of Boc- and Pht-protected diene substrates for endoperoxide synthesis. TBA-Cl = tetrabuty...
Scheme 3: Synthesis of endoperoxides 17–19 by [4 + 2]-cycloaddition of dienes 14–16 with singlet oxygen. The ...
Scheme 4: Dihydroxylation and protection of endoperoxides 18 and 19 to provide novel building blocks 20–23 fo...
Beilstein J. Org. Chem. 2013, 9, 1383–1387, doi:10.3762/bjoc.9.154
Figure 1: Marketed calcium-sensing receptor agonist cinacalcet (1), and CaSR antagonists Calhex 231 (2) and N...
Scheme 1: Strategy for assembling (R)-3 from fragments 4, 5 and 6. m-Ns = m-nitrobenzenesulfonyl.
Scheme 2: Synthesis of amine building block 6 by using Katritzky’s pyrylium chemistry [16].
Scheme 3: Synthesis of phenol 4 from commercially available aryl fluoride 13.
Scheme 4: Synthesis of rac-3 and (R)-3 from commercially available racemic- and (S)-glycidol 15, respectively...
Figure 2: Determination of the optical purity for (R)-3 by chiral HPLC on a Daicel AD-H column. Top: Opticall...
Figure 3: Characterisation of concentration-dependent (R)-3 inhibition of 3.5 mM calcium-stimulated IP1 respo...